DIN ISO 10382 E : 2003
Current
The latest, up-to-date edition.
SOIL QUALITY - DETERMINATION OF ORGANOCHLORINE PESTICIDES AND POLYCHLORINATED BIPHENYLS - GAS-CHROMATOGRAPHIC METHOD WITH ELECTRON CAPTURE DETECTION
Hardcopy , PDF
English
01-01-2003
Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Preparation of standard solutions of PCB and OCP
7 Sampling and preservation of samples
7.1 Sampling
7.2 Sample preservation and pretreatment
8 Procedure
8.1 Blank
8.2 Extraction and concentration
8.3 Clean-up of the extract
8.4 Column-chromatographic separation of PCBs and
non-polar OCPs from several polar OCPs
8.5 Gas chromatographic analysis
9 Test report
10 Accuracy
Annex A (informative) Table of retention times
of polychlorinated biphenyls and organochlorine
pesticides for two different capillary columns
Annex B (informative) Scheme for the preparation of standard
solutions including injection Standards
Annex C (informative) Results of an interlaboratory trial
carried out in the Netherlands
Annex D (informative) Clean-up to remove elemental sulfur
and some other organic sulfur compounds
Bibliography
Access your standards online with a subscription
Features
-
Simple online access to standards, technical information and regulations.
-
Critical updates of standards and customisable alerts and notifications.
-
Multi-user online standards collection: secure, flexible and cost effective.