BS 6068-2.99(2006) : 2006
Current
The latest, up-to-date edition.
WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENYL ETHERS IN SEDIMENT AND SEWAGE SLUDGE - METHOD USING EXTRACTION AND GAS CHROMATOGRAPHY/MASS SPECTROMETRY
Hardcopy , PDF
English
01-01-2006
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents and standards
6 Apparatus
7 Sampling and sample pre-treatment
8 Procedure
9 Calibration
10 Test report
Annex A (informative) - Clean-up procedures
Annex B (informative) - Examples for separation conditions
in gas chromatography and mass spectrometry
Annex C (informative) - Typical ions and time windows for
electron impact ionization detection
Annex D (informative) - Examples of chromatograms and spectra
Annex E (informative) - Precision data
Bibliography
Defines a method for the determination of selected polybrominated diphenyl ethers (PBDE) in sediment and sludge using gas chromatography/mass spectrometry (GC-MS) in the electron impact (EI) or negative ion chemical ionization (NCI) mode.
| Committee |
EH/3/2
|
| DevelopmentNote |
Supersedes 04/30091620 DC. (02/2007) Also numbered as BS EN ISO 22032. (06/2009)
|
| DocumentType |
Standard
|
| Pages |
36
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| EN ISO 22032:2009 | Identical |
| ISO 22032:2006 | Identical |
| ISO 5667-13:2011 | Water quality — Sampling — Part 13: Guidance on sampling of sludges |
| ISO/TR 13530:1997 | Water quality — Guide to analytical quality control for water analysis |
| EN 12880:2000 | Characterization of sludges - Determination of dry residue and water content |
| DIN 32645:2008-11 | CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ISO 8466-1:1990 | Water quality — Calibration and evaluation of analytical methods and estimation of performance characteristics — Part 1: Statistical evaluation of the linear calibration function |
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