BS ISO 11709:2011
Current
The latest, up-to-date edition.
Soil quality. Determination of selected coal-tar-derived phenolic compounds using high performance liquid chromatography (HPLC)
Hardcopy , PDF
English
31-05-2011
Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Reagents
7 Apparatus
8 Sampling and preservation of samples
9 Procedure
10 Calculation and expression of results
11 Test report
Annex A (informative) - Example of chromatographic conditions
and chromatogram
Annex B (informative) - Emission spectrum (FLD, 280 nm to
900 nm) recorded with FLD Agilent 1100
Annex C (informative) - Ultraviolet spectrum (DAD, 200 nm to
350 nm), recorded with Dionex UVD 320S
Annex D (informative) - Examples of limits of determinations
of coal-tar-derived phenols for different HPLC detectors
Bibliography
Describes a method for the quantitative determination of selected coal-tar-derived phenols, namely phenol, methylphenols such as (ortho-, meta-, para-)cresols, and dihydroxybenzenes such as catechol, resorcinol and hydroquinone in soil by using high performance liquid chromatography with ultraviolet/diode array (HPLC/UV/DAD) or fluorescence (HPLC/FLD) or electrochemical detection (HPLC/ELCD).
| Committee |
EH/4
|
| DocumentType |
Standard
|
| Pages |
30
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
This International Standard specifies a method for the quantitative determination of selected coal-tar-derived phenols, namely phenol, methylphenols such as (ortho-, meta-, para-)cresols, and dihydroxybenzenes such as catechol, resorcinol and hydroquinone (see Table1) in soil by using high performance liquid chromatography with ultraviolet/diode array (HPLC/UV/DAD) or fluorescence (HPLC/FLD) or electrochemical detection (HPLC/ELCD). It is applicable to all types of soil with contamination levels of individual phenols in the range of approximately 0,08mg/kg to 10mg/kg of soil.
NOTE Also with this method, other higher methylated phenols, for example, dimethylphenols such as (2,3-, 2,4-, 2,5-, 2,6-, 3,4- and 3,5-)xylenoles, 2-isopropylphenol, 2,3,5-trimethylphenol and 1-naphthol can be analysed, provided the suitability and the validity of the method are proven.
| Standards | Relationship |
| ISO 11709:2011 | Identical |
| ISO 16072:2002 | Soil quality — Laboratory methods for determination of microbial soil respiration |
| ISO 10381-1:2002 | Soil quality — Sampling — Part 1: Guidance on the design of sampling programmes |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| ISO 648:2008 | Laboratory glassware — Single-volume pipettes |
| ISO 10381-2:2002 | Soil quality — Sampling — Part 2: Guidance on sampling techniques |
| DIN 32645:2008-11 | CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION |
| ISO 8466-1:1990 | Water quality — Calibration and evaluation of analytical methods and estimation of performance characteristics — Part 1: Statistical evaluation of the linear calibration function |
| ISO 14154:2005 | Soil quality — Determination of some selected chlorophenols — Gas-chromatographic method with electron-capture detection |
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