ISO 16362:2005
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Ambient air — Determination of particle-phase polycyclic aromatic hydrocarbons by high performance liquid chromatography
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English
18-02-2005
ISO 16362:2005 specifies sampling, cleanup and analysis procedures for the quantitative determination of low volatility (particle-bound) polycyclic aromatic hydrocarbons (PAHs) in ambient air. For sampling, a low-volume or a medium/high-volume sampling device may be used. Sampling times between 1 h and 24 h are possible. The sampling volume flow rates can range from 1 m/h to 4 m/h ("low volume sampler") or from 10 m/h to about 90 m/h ("medium/high-volume sampler"). In any case, the linear face velocity at the collection filter should range between about 0,5 m/s and 0,9 m/s.
The method has been validated for sampling periods up to 24 h. The detection limits for single PAHs and the standard deviations resulting from duplicate measurements are listed.
ISo 16362:2005 describes a sampling and analysis procedure for PAH that involves collection from air onto a filter followed by analysis using high performance liquid chromatography usually with fluorescence detector (FLD). The use of a diode array detector (DAD) is possible. The combination of both detector types is also possible. Total suspended particulate matter is sampled.
Generally, compounds having a boiling point above 430 °C (vapour pressure less than 10-9 kPa at 25 °C, e.g. chrysene, benz[a]anthracene) can be collected efficiently on the filter at low ambient temperatures (e.g. below 10 °C). In contrast, at higher temperatures (above 30 °C, see also ISO 12884[1]), only PAHs having boiling points above 475 °C (vapour pressure less than 10-10 kPa at 25 °C) are determined quantitatively.
| DevelopmentNote |
Supersedes ISO/DIS 16362 (02/2005)
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| DocumentType |
Standard
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| Pages |
27
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| ProductNote |
THIS STANDARD ALSO REFERS TO NIST Special Publication 922
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| PublisherName |
International Organization for Standardization
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| Status |
Current
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| Standards | Relationship |
| DIN ISO 16362:2006-01 | Identical |
| BS ISO 16362:2005 | Identical |
| GOST R ISO 16362 : 2009 | Identical |
| UNE-ISO 16362:2006 | Identical |
| DIN EN 15980:2011-08 | Air quality - Determination of the deposition of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene, dibenz[a,h]anthracene and indeno[1,2,3-cd]pyrene |
| 06/30146327 DC : 0 | EN ISO 16000-12 - INDOOR AIR - PART 12: SAMPLING STRATEGY FOR POLYCYCLIC AROMATIC HYDROCARBONS (PAHS), POLYCHLORINATED DIBENZO-P-DIOXINS (PCDDS), POLYCHLORINATED DIBENZO-FURANS (PCDFS) AND POLYCHLORINATED BIPHENYLS (PCBS) |
| I.S. EN ISO 16000-12:2008 | INDOOR AIR - PART 12: SAMPLING STRATEGY FOR POLYCHLORINATED BIPHENYLS (PCBS), POLYCHLORINATED DIBENZO-P-DIOXINS (PCDDS), POLYCHLORINATED DIBENZOFURANS (PCDFS) AND POLYCYCLIC AROMATIC HYDROCARBONS (PAHS) |
| DIN EN 15549:2008-06 | Air quality - Standard method for the measurement of the concentration of benzo[a]pyrene in ambient air |
| NF EN ISO 16000-12 : 2009 | INDOOR AIR - PART 12: SAMPLING STRATEGY FOR POLYCHLORINATED BIPHENYLS (PCBS), POLYCHLORINATED DIBENZO-P-DIOXINS (PCDDS), POLYCHLORINATED DIBENZOFURANS (PCDFS) AND POLYCYCLIC AROMATIC HYDROCARBONS (PAHS) |
| BS EN 15549:2008 | Air quality. Standard method for the measurement of the concentration of benzo(a)pyrene in ambient air |
| S.R. CEN/TS 16645:2014 | AMBIENT AIR - METHOD FOR THE MEASUREMENT OF BENZ[A]ANTHRACENE, BENZO[B]FLUORANTHENE, BENZO[J]FLUORANTHENE, BENZO[K]FLUORANTHENE, DIBENZ[A,H]ANTHRACENE, INDENO[1,2,3-CD]PYRENE AND BENZO[GHI]PERYLENE |
| VDI 4301 Blatt 7:2017-04 (Draft) | Measurement of indoor air pollution - Measurement of carboxylic acids |
| VDI 4301 Blatt 5:2009-04 | Measurement of indoor air pollution - Measurement of flame retardants and plasticizers based on organophosphorous compounds - Phosphoric acid ester |
| VDI 4301 Blatt 6:2012-09 | Measurement of indoor air pollution - Measurement of phthalates with GC/MS |
| 09/30193287 DC : 0 | BS EN 15980 - AIR QUALITY - DETERMINATION OF THE DEPOSITION OF BENZ[A]ANTHRACENE, BENZO[B]FLUORANTHENE, BENZO[J]FLUORANTHENE, BENZO[K]FLUORANTHENE, BENZO[A]PYRENE, DIBENZ[A,H]ANTHRACENE AND INDENO[1,2,3-CD]PYRENE |
| BS EN 15980:2011 | Air quality. Determination of the deposition of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene, dibenz[a,h]anthracene and indeno[1,2,3-cd]pyrene |
| DIN EN ISO 16000-12:2008-08 | INDOOR AIR - PART 12: SAMPLING STRATEGY FOR POLYCHLORINATED BIPHENYLS (PCBS), POLYCHLORINATED DIBENZO-P-DIOXINS (PCDDS), POLYCHLORINATED DIBENZOFURANS (PCDFS) AND POLYCYCLIC AROMATIC HYDROCARBONS (PAHS) |
| I.S. EN 15980:2011 | AIR QUALITY - DETERMINATION OF THE DEPOSITION OF BENZ[A]ANTHRACENE, BENZO[B]FLUORANTHENE, BENZO[J]FLUORANTHENE, BENZO[K]FLUORANTHENE, BENZO[A]PYRENE, DIBENZ[A,H]ANTHRACENE AND INDENO[1,2,3-CD]PYRENE |
| I.S. EN 15549:2008 | AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF THE CONCENTRATION OF BENZO[A]PYRENE IN AMBIENT AIR |
| BS EN ISO 16000-12:2008 | Indoor air Sampling strategy for polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polycyclic aromatic hydrocarbons (PAHs) |
| PD CEN/TS 16645:2014 | Ambient air. Method for the measurement of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, dibenz[a,h]anthracene, indeno[1,2,3-cd]pyrene and benzo[ghi]perylene |
| ISO 16000-12:2008 | Indoor air — Part 12: Sampling strategy for polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polycyclic aromatic hydrocarbons (PAHs) |
| EN ISO 16000-12:2008 | Indoor air - Part 12: Sampling strategy for polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polycyclic aromatic hydrocarbons (PAHs) (ISO 16000-12:2008) |
| EN 15980:2011 | Air quality - Determination of the deposition of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene, dibenz[a,h]anthracene and indeno[1,2,3-cd]pyrene |
| EN 15549:2008 | Air quality - Standard method for the measurement of the concentration of benzo[a]pyrene in ambient air |
| CEN/TS 16645:2014 | Ambient air - Method for the measurement of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, dibenz[a,h]anthracene, indeno[1,2,3-cd]pyrene and benzo[ghi]perylene |
| UNE-EN 15980:2011 | Air quality - Determination of the deposition of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, benzo[a]pyrene, dibenz[a,h]anthracene and indeno[1,2,3-cd]pyrene |
| ISO 12884:2000 | Ambient air — Determination of total (gas and particle-phase) polycyclic aromatic hydrocarbons — Collection on sorbent-backed filters with gas chromatographic/mass spectrometric analyses |
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