PREN 15308 : DRAFT 2015
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
09-03-2016
01-10-2016
European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Safety precautions
8 Interferences
9 Sample storage
10 Pretreatment
11 Procedure
12 Calculation
13 Test report
Annex A (informative) - Performance characteristics
Annex B (informative) - Examples of GC-MS chromatograms
of a calibration standard solution and a contaminated
soil sample
Annex C (informative) - Examples of GC-ECD chromatograms
of a calibration standard solution and a cable
shredder sample
Annex D (normative) - Calculation method for the estimation
of total PCB content
Annex E (informative) - Summary of general requirements and
Recommendations
Bibliography
Defines a method for quantitative determination of seven polychlorinated biphenyl congeners (PCB-28, PCB-52, PCB-101, PCB-118, PCB-138, PCB-153 and PCB-180) in solid waste using high-resolution gas chromatography with electron capture or mass spectrometric detection.
| Committee |
TC 292
|
| DocumentType |
Draft
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Superseded
|
| SupersededBy |
| Standards | Relationship |
| 15/30330799 DC : 0 | Identical |
| 05/30136951 DC : 0 | Identical |
| EN ISO 6468:1996 | Water quality - Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes - Gas chromatographic method after liquid-liquid extraction (ISO 6468:1996) |
| EN 12766-1:2000 | Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD) |
| ISO 11464:2006 | Soil quality — Pretreatment of samples for physico-chemical analysis |
| ISO 22892:2006 | Soil quality — Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| EN 61619:1997 | Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography |
| EN 14346:2006 | Characterization of waste - Calculation of dry matter by determination of dry residue or water content |
| ISO 14507:2003 | Soil quality — Pretreatment of samples for determination of organic contaminants |
| EN 12766-2:2001 | Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| EN ISO 22892:2011 | Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006) |
| IEC 61619:1997 | Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography |
| ISO 6468:1996 | Water quality — Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes — Gas chromatographic method after liquid-liquid extraction |