PREN 17212 : DRAFT 2017
Current
The latest, up-to-date edition.
ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALSYSIS - DETERMINATION OF MELAMINE AND CYANURIC ACID CONTENT BYLIQUID CHROMATOGRAPHIC METHOD WITH MASS SPECTROMETRIC DETECTION (LC-MS/MS)
09-01-2018
European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Preparation of sample
8 Procedure
9 HPLC-MS/MS analysis
10 Calculation
11 Precision
12 Test report
Annex A (informative) - Examples for suitable MS detection
conditions
Annex B (informative) - Results of the international
collaborative trial
Annex C (informative) - Results of the in-house validation
of the method
Annex D (informative) - Typical chromatograms
Bibliography
Provides a high-performance liquid chromatographic (HPLC) mass spectrometric (MS) method for screening and quantification of melamine in the concentration range between < 1 mg/kg and 100 mg/kg feed.
| Committee |
TC 327
|
| DocumentType |
Draft
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Standards | Relationship |
| NEN EN 17212 : DRAFT 2018 | Identical |
| DIN EN 17212:2018-01 (Draft) | Identical |
| 17/30337117 DC : DRAFT DEC 2017 | Identical |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| ISO 11843-2:2000 | Capability of detection — Part 2: Methodology in the linear calibration case |
| ISO 24276:2006 | Foodstuffs — Methods of analysis for the detection of genetically modified organisms and derived products — General requirements and definitions |
| EN ISO/IEC 17043:2010 | Conformity assessment - General requirements for proficiency testing (ISO/IEC 17043:2010) |
| ISO 6497:2002 | Animal feeding stuffs — Sampling |
| ISO/IEC Guide 99:2007 | International vocabulary of metrology — Basic and general concepts and associated terms (VIM) |
| ISO 3534-2:2006 | Statistics — Vocabulary and symbols — Part 2: Applied statistics |
| ISO/IEC 17043:2010 | Conformity assessment — General requirements for proficiency testing |
| EN ISO 6498:2012 | Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012) |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| EN ISO 6497:2005 | Animal feeding stuffs - Sampling (ISO 6497:2002) |
| ISO 6498:2012 | Animal feeding stuffs — Guidelines for sample preparation |
| ISO 16577:2016 | Molecular biomarker analysis — Terms and definitions |