AS ISO 15472-2006

1 - AS ISO 15472-2006 Surface chemical analysis - X-ray photoelectron spectrometers - Calibration of energy scales
4 - PREFACE
5 - CONTENTS
6 - INTRODUCTION
7 - 1 Scope
7 - 2 Normative reference
7 - 3 Symbols and abbreviated terms
8 - 4 Outline of method
12 - 5 Procedure for calibrating the energy scale
12 - 5.1 Obtaining the reference samples
12 - 5.2 Mounting the samples
12 - 5.3 Cleaning the samples
12 - 5.4 Choosing the spectrometer settings for which energy calibration is required
12 - 5.5 Operating the instrument
13 - 5.6 Options for initial or subsequent calibration measurements
13 - 5.7 Measurements for the peak binding-energy repeatability standard deviation and the scale linearity
14 - 5.8 Calculating the peak binding-energy repeatability standard deviation
17 - 5.9 Checking the binding-energy scale linearity
18 - 5.10 Procedure for the regular determination of the calibration error
19 - 5.11 Procedures for correction of the instrument binding-energy scale
21 - 5.12 Next calibration
21 - 5.13 Establishing the calibration interval
22 - Annex A (normative) Least-squares determination of the peak binding energy by a simple computational method
25 - Annex B (informative) Derivation of uncertainties
27 - Annex C (informative) Citation of the uncertainties of measured binding energies
29 - Annex D (informative) Measurements of modified Auger parameters measured using XPS instruments equipped with a monochromated Al X-ray source
32 - Bibliography

Adopts ISO 15472:2001 to specify a method for calibrating the binding-energy scales of X-ray photoelectron spectrometers for general analytical purposes.

First published as AS ISO 15472-2006.