EN ISO 3838:2004

Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
   4.1 Capillary-stoppered pyknometer
   4.2 Graduated bicapillary pyknometer
5 Apparatus
6 Preparation of pyknometer
7 Calibration of pyknometer
   7.1 Conditioning
   7.2 Capillary-stoppered pyknometer
   7.3 Graduated bicapillary pyknometer
   7.4 Other reference temperatures
   7.5 Recalibration
8 Procedure for capillary-stoppered pyknometers
   8.1 Procedure for liquids
   8.2 Procedure for solid or semi-solid sample
9 Procedure for graduated bicapillary pyknometers
10 Calculation
   10.1 Symbols
   10.2 Reference, calibration and test temperatures
   10.3 Correction for the thermal expansion of the pyknometer
   10.4 Calculation of density of a liquid
   10.5 Calculation of relative density of liquid
   10.6 Calculation of density or relative density of a solid
        or semi-solid
11 Precision
   11.1 Capillary-stoppered pyknometer method
   11.2 Graduated bicapillary pyknometer method
12 Test report

ISO 3838:2004 specifies methods for the determination of the density or relative density of crude petroleum and of petroleum products handled as liquids.The capillary-stoppered pyknometer method is also for use with solids and this method may also be used for coal tar products, including road tars, creosote and tar pitches, or for mixtures of these with petroleum products. This method is not suitable for the determination of the density or relative density of highly volatile liquids having Reid vapour pressures greater than 50 kPa according to ISO 3007 or having an initial boiling point below 40 degrees Celsius.The graduated bicapillary pyknometer method is recommended for the accurate determination of the density or relative density of all except the more viscous products, and is particularly useful when only small amounts of samples are available. The method is restricted to liquids having Reid vapour pressures of 130 kPa or less according to ISO 3007 and having kinematic viscosities less than 50 mm2/s (50 centistokes (cSt)) at the test temperature.Special precautions are specified for the determination of the density or relative density of highly volatile liquids.