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ASTM D 5847 : 2002 : R2012

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
Available format(s)

Hardcopy , PDF

Superseded date

08-08-2020

Language(s)

English

Published date

10-18-2012

This practice provides specific, mandatory requirements for incorporating quality control (QC) procedures into all test methods under the jurisdiction of Committee D-19.

1.1 This practice provides specific, mandatory requirements for incorporating quality control (QC) procedures into all test methods under the jurisdiction of Committee D-19.

1.2 ASTM has adopted the following:

Policy on implementation of requirements for a quality control section in standard test methods generated by Committee D-19 on Water.
GENERALBy July 29, 1998, or at the next reapproval or revision, whichever is later, every D-19 Standard Test Method shall contain a QC section that is in full compliance with the requirements of this practice.
NEW COLLABORATIVE TESTINGAs of July 29, 1998, each collaborative study design shall include a QC section as part of the method to be tested. Prior to approval of the study design, the Results Advisor shall ascertain the appropriateness of the QC section in meeting the requirements of this Practice and Practice D2777, and shall advise the designer of the study of any changes needed to fulfill the requirements of these practices. Before a collaborative study may be conducted, approval of the study design by the Results Advisor must be obtained.
OLDER VALIDATED METHODSStandard test methods that were validated using D-2777-77, D-2777-86, or D-2777-94, when ballotted for reapproval or revision, shall contain a QC section based upon the best information from the historical record. Where appropriate, information derived from the record of the collaborative study shall be utilized for this purpose. The introduction of the QC section into these standard test methods shall not be construed as a requirement for a new collaborative study, though the Subcommittee may opt for such a study. Any information available regarding QC or precision/bias testing shall be included in the appropriate sections of the published method.

1.3 Required QC sections in all applicable test methods are intended to achieve two goals. First, users of Committee D-19 test methods will be able to demonstrate a minimum competency in the performance of these test methods by comparison with collaborative study data. Second, all users of test methods will be required to perform a minimum level of QC as part of proper implementation of these test methods to ensure ongoing competency.

1.4 This practice contains the primary requirements for QC of a specific test method. In many cases, it may be desirable to implement additional QC requirements to assure the desired quality of data.

1.5 The specific requirements in this practice may not be applicable to all test methods. These requirements may vary depending on the type of test method used as well as the analyte being determined and the sample matrix being analyzed. See Explanation 1 in Appendix X1.

1.5.1 If there are compelling reasons why any of the specific QC requirements listed in this practice are not applicable to a specific test method, these reasons must be documented in the QC section of the test method.

1.5.2 With the approval of Committee D-19 on the recommendation of the D-19 Results Advisor and the Technical Operations section of the Executive Subcommittee, a statement giving the compelling reasons why compliance with all or specific points of this practice cannot be achieved will meet the requirements of both ASTM and this practice.

1.5.3 Test Methods developed prior to the approval of this practice with a QC Section that meet the requirements of Specification D5789 are considered in compliance with this Practice.

1.6 This practice is for use with quantitative methods and may not be applicable to qualitative test methods.

1.7 Presently, this practice is applicable primarily to chemical test methods. It is intended that, in future revisions, the practice will be expanded to include other methods such as microbiological methods.

Committee
D 19
DevelopmentNote
Supersedes ASTM D 5789. (09/2002)
DocumentType
Standard Practice
Pages
11
ProductNote
Reconfirmed 2012
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

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ASTM D 7599 : 2016 : R2017 Standard Test Method for Determination of Diethanolamine, Triethanolamine, <emph type="ital">N</emph>-Methyldiethanolamine and <emph type="ital">N</emph >-Ethyldiethanolamine in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 1886 : 2014 Standard Test Methods for Nickel in Water
ASTM D 4165 : 2006 : R2020 : EDT 1 Standard Test Method for Cyanogen Chloride in Water
ASTM D 1976 : 2019 Standard Test Method for Elements in Water by Inductively-Coupled Plasma Atomic Emission Spectroscopy
ASTM D 1252 : 2006 : R2020 Standard Test Methods for Chemical Oxygen Demand (Dichromate Oxygen Demand) of Water
ASTM D 1783 : 2001 : R2020 Standard Test Methods for Phenolic Compounds in Water
ASTM D 8018 : 2015 : R2020 Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Soil by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS)
ASTM D 2330 : 2020 Standard Test Method for Methylene Blue Active Substances
ASTM D 7979 : 2019 Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances in Water, Sludge, Influent, Effluent, and Wastewater by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 8064 : 2016 Standard Test Method for Elemental Analysis of Soil and Solid Waste by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry Using Multiple Monochromatic Excitation Beams
ASTM D 1067 : 2016 Standard Test Methods for Acidity or Alkalinity of Water
ASTM D 7283 : 2017 Standard Test Method for Alpha and Beta Activity in Water By Liquid Scintillation Counting
ASTM D 4165 : 2006 : R2012 Standard Test Method for Cyanogen Chloride in Water
ASTM D 4922 : 2009 : R2016 : EDT 1 Standard Test Method for Determination of Radioactive Iron in Water
ASTM D 7597 : 2016 : R2017 Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Hydrogen Dimethylamidophosphate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Water by Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 857 : 2017 Standard Test Method for Aluminum in Water
ASTM D 8025 : 2016 Standard Test Method for Determination of Select Pesticides in Water by Multiple Reaction Monitoring Liquid Chromatography Tandem Mass Spectrometry
ASTM D 3697 : 2017 Standard Test Method for Antimony in Water
ASTM D 7485 : 2016 Standard Test Method for Determination of Nonylphenol, p-<emph type="bdit">tert</emph >-Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 5072 : 2009 : R2016 Standard Test Method for Radon in Drinking Water
ASTM D 3373 : 2017 Standard Test Method for Vanadium in Water
ASTM D 3082 : 2015 Standard Test Method for Boron in Water
ASTM D 7535 : 2009 : R2015 Standard Test Method for Lead-210 in Water (Withdrawn 2024)
ASTM D 516 : 2016 Standard Test Method for Sulfate Ion in Water
ASTM D 6855 : 2017 Standard Test Method for Determination of Turbidity Below 5 NTU in Static Mode
ASTM D 6501 : 2015 Standard Test Method for Phosphonate in Brines
ASTM D 1783 : 2001 : R2012 : EDT 1 Standard Test Methods for Phenolic Compounds in Water
ASTM D 7644 : 2016 Standard Test Method for Determination of Bromadiolone, Brodifacoum, Diphacinone and Warfarin in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 1126 : 2017 Standard Test Method for Hardness in Water
ASTM D 4691 : 2017 Standard Practice for Measuring Elements in Water by Flame Atomic Absorption Spectrophotometry
ASTM D 5811 : 2008 : R2013 Standard Test Method for Strontium-90 in Water
ASTM D 4191 : 2015 Standard Test Method for Sodium in Water by Atomic Absorption Spectrophotometry
ASTM D 8026 : 2016 Standard Practice for Determination of Tc-99 in Water by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
ASTM D 513 : 2016 Standard Test Methods for Total and Dissolved Carbon Dioxide in Water
ASTM D 7678 : 2017 Standard Test Method for Total Oil and Grease (TOG) and Total Petroleum Hydrocarbons (TPH) in Water and Wastewater with Solvent Extraction using Mid-IR Laser Spectroscopy
ASTM D 5673 : 2016 Standard Test Method for Elements in Water by Inductively Coupled Plasma—Mass Spectrometry
ASTM D 512 : 2012 Standard Test Methods for Chloride Ion In Water (Withdrawn 2021)
ASTM D 7284 : 2013 : R2017 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 5904 : 2002 : R2017 Standard Test Method for Total Carbon, Inorganic Carbon, and Organic Carbon in Water by Ultraviolet, Persulfate Oxidation, and Membrane Conductivity Detection
ASTM D 3865 : 2009 : R2015 Standard Test Method for Plutonium in Water (Withdrawn 2024)
ASTM D 7511 : 2012 : R2017 : EDT 1 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
ASTM D 7237 : 2018 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 3645 : 2015 Standard Test Methods for Beryllium in Water
ASTM D 4282 : 2015 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 5174 : 2007 : R2013 Standard Test Method for Trace Uranium in Water by Pulsed-Laser Phosphorimetry (Withdrawn 2022)
ASTM D 4658 : 2015 Standard Test Method for Sulfide Ion in Water (Withdrawn 2024)
ASTM D 4193 : 2008 : R2013 : EDT 1 Standard Test Method for Thiocyanate in Water
ASTM D 6994 : 2015 Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
ASTM D 4327 : 2017 Standard Test Method for Anions in Water by Suppressed Ion Chromatography
ASTM D 4190 : 2015 Standard Test Method for Elements in Water by Direct-Current Plasma Atomic Emission Spectroscopy
ASTM D 7365 : 2009 : REV A : R2015 Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
ASTM D 7315 : 2017 Standard Test Method for Determination of Turbidity Above 1 Turbidity Unit (TU) in Static Mode
ASTM D 3972 : 2009 : R2015 Standard Test Method for Isotopic Uranium in Water by Radiochemistry (Withdrawn 2024)
ASTM D 7968 : 2017 : REV A Standard Test Method for Determination of Polyfluorinated Compounds in Soil by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM D 7742 : 2017 Standard Practice for Determination of Nonylphenol Polyethoxylates (NPnEO, 3 ≤ n ≤ 18) and Octylphenol Polyethoxylates (OPnEO, 2 ≤ n ≤ 12) in Water by Single Reaction Monitoring (SRM) Liquid Chromatography/ Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 3651 : 2016 Standard Test Method for Barium in Brackish Water, Seawater, and Brines
ASTM D 1068 : 2015 Standard Test Methods for Iron in Water
ASTM D 859 : 2016 Standard Test Method for Silica in Water
ASTM D 4458 : 2015 Standard Test Method for Chloride Ions in Brackish Water, Seawater, and Brines
ASTM D 7645 : 2016 Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 7598 : 2016 : R2017 Standard Test Method for Determination of Thiodiglycol in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 3454 : 2018 Standard Test Method for Radium-226 in Water
ASTM D 7065 : 2017 Standard Test Method for Determination of Nonylphenol, Bisphenol A, <emph type="bdit" >p-tert</emph>-Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Gas Chromatography Mass Spectrometry
ASTM D 3561 : 2016 Standard Test Method for Lithium, Potassium, and Sodium Ions in Brackish Water, Seawater, and Brines by Atomic Absorption Spectrophotometry
ASTM D 5257 : 2017 Standard Test Method for Dissolved Hexavalent Chromium in Water by Ion Chromatography
ASTM D 8018 : 2015 Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Soil by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS)
ASTM D 3223 : 2017 Standard Test Method for Total Mercury in Water
ASTM D 3867 : 2016 Standard Test Methods for Nitrite-Nitrate in Water
ASTM D 3868 : 2015 Standard Test Method for Fluoride Ions in Brackish Water, Seawater, and Brines
ASTM D 2036 : 2009 : R2015 Standard Test Methods for Cyanides in Water
ASTM D 8024 : 2016 Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Water by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS)
ASTM D 4785 : 2008 : R2013 : EDT 1 Standard Test Method for Low-Level Analysis of Iodine Radioisotopes in Water
ASTM D 8243 : 2019 Standard Test Method for Determination of APS Reductase to Estimate Sulfate Reducing Bacterial Bioburdens in Water – Enzyme-Linked Immunosorbent Assay Method
ASTM D 1429 : 2013 Standard Test Methods for Specific Gravity of Water and Brine (Withdrawn 2022)
ASTM D 6238 : 1998 : R2017 Standard Test Method for Total Oxygen Demand in Water
ASTM D 4192 : 2015 Standard Test Method for Potassium in Water by Atomic Absorption Spectrophotometry
ASTM D 8083 : 2016 Standard Test Method for Total Nitrogen, and Total Kjeldahl Nitrogen (TKN) by Calculation, in Water by High Temperature Catalytic Combustion and Chemiluminescence Detection
ASTM D 6239 : 2009 : R2015 Standard Test Method for Uranium in Drinking Water by High-Resolution Alpha-Liquid-Scintillation Spectrometry (Withdrawn 2024)
ASTM D 858 : 2017 Standard Test Methods for Manganese in Water
ASTM D 6919 : 2017 Standard Test Method for Determination of Dissolved Alkali and Alkaline Earth Cations and Ammonium in Water and Wastewater by Ion Chromatography
ASTM D 1385 : 2007 : R2018 : EDT 1 Standard Test Method for Hydrazine in Water
ASTM D 7574 : 2016 Standard Test Method for Determination of Bisphenol A in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 3372 : 2017 Standard Test Method for Molybdenum in Water
ASTM D 511 : 2014 Standard Test Methods for Calcium and Magnesium In Water
ASTM D 3559 : 2015 Standard Test Methods for Lead in Water (Withdrawn 2024)
ASTM D 4839 : 2003 : R2017 Standard Test Method for Total Carbon and Organic Carbon in Water by Ultraviolet, or Persulfate Oxidation, or Both, and Infrared Detection
ASTM D 7939 : 2015 Standard Test Method for Rapid Radiochemical Determination of Americium-241 in Water (Withdrawn 2024)
ASTM D 7575 : 2011 : R2017 Standard Test Method for Solvent-Free Membrane Recoverable Oil and Grease by Infrared Determination
ASTM D 8193 : 2018 Standard Test Method for Total Oil and Grease (TOG) and Total Petroleum Hydrocarbon (TPH) in Water and Wastewater with Solvent Extraction Using Non-Dispersive Mid-IR Transmission Spectroscopy
ASTM D 2777 : 2013 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3352 : 2015 Standard Test Method for Strontium Ion in Brackish Water, Seawater, and Brines
ASTM D 7168 : 2016 Standard Test Method for <sup>99</sup>Tc in Water by Solid Phase Extraction Disk
ASTM D 8001 : 2016 : EDT 1 Standard Test Method for Determination of Total Nitrogen, Total Kjeldahl Nitrogen by Calculation, and Total Phosphorus in Water, Wastewater by Ion Chromatography
ASTM D 1691 : 2017 Standard Test Methods for Zinc in Water
ASTM D 1246 : 2016 Standard Test Method for Bromide Ion in Water
ASTM D 3590 : 2017 Standard Test Methods for Total Kjeldahl Nitrogen in Water
ASTM D 4012 : 2015 Standard Test Method for Adenosine Triphosphate (ATP) Content of Microorganisms in Water
ASTM D 7066 : 2004 : R2017 Standard Test Method for dimer/trimer of chlorotrifluoroethylene (S-316) Recoverable Oil and Grease and Nonpolar Material by Infrared Determination
ASTM D 3986 : 2017 Standard Test Method for Barium in Brines, Seawater, and Brackish Water by Direct-Current Argon Plasma Atomic Emission Spectroscopy
ASTM D 1179 : 2016 Standard Test Methods for Fluoride Ion in Water
ASTM D 7572 : 2015 Standard Guide for Recovery of Aqueous Cyanides by Extraction from Mine Rock and Soil
ASTM D 3875 : 2015 Standard Test Method for Alkalinity in Brackish Water, Seawater, and Brines
ASTM D 6071 : 2014 Standard Test Method for Low Level Sodium in High Purity Water by Graphite Furnace Atomic Absorption Spectroscopy
ASTM D 5996 : 2016 Standard Test Method for Measuring Anionic Contaminants in High-Purity Water by On-Line Ion Chromatography
ASTM D 3919 : 2015 Standard Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption Spectrophotometry
ASTM D 1426 : 2015 Standard Test Methods for Ammonia Nitrogen In Water
ASTM D 3557 : 2017 Standard Test Methods for Cadmium in Water
ASTM D 2460 : 2007 : R2013 Standard Test Method for Alpha-Particle-Emitting Isotopes of Radium in Water (Withdrawn 2022)
ASTM D 7600 : 2016 : R2017 Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 3558 : 2015 Standard Test Methods for Cobalt in Water
ASTM D 5542 : 2016 Standard Test Methods for Trace Anions in High Purity Water by Ion Chromatography
ASTM D 6888 : 2016 Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 4130 : 2015 Standard Test Method for Sulfate Ion in Brackish Water, Seawater, and Brines (Withdrawn 2024)

ASTM D 3648 : 2004 : R2011 Standard Practices for the Measurement of Radioactivity
ASTM D 1129 : 2013 : REDLINE Standard Terminology Relating to Water
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM D 2777 : 2013 : REDLINE Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 4375 : 1996 : R2001 Standard Practice for Basic Statistics in Committee D-19 on Water
ASTM D 5810 : 1996 : R2011 Standard Guide for Spiking into Aqueous Samples
ASTM D 2777 : 2012 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 4375 : 1996 Standard Practice for Basic Statistics in Committee D-19 on Water
ASTM D 5810 : 1996 : R2001 Standard Guide for Spiking into Aqueous Samples
ASTM D 4375 : 1996 : R2006 Standard Practice for Basic Statistics in Committee D-19 on Water
ASTM D 3648 : 2014 : REDLINE Standard Practices for the Measurement of Radioactivity (Withdrawn 2023)
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM D 3648 : 2014 Standard Practices for the Measurement of Radioactivity (Withdrawn 2023)
ASTM D 2777 : 2003 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
ASTM D 3648 : 2003 Standard Practices for the Measurement of Radioactivity
ASTM D 2777 : 2013 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3648 : 2004 Standard Practices for the Measurement of Radioactivity
ASTM D 2777 : 1998 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
ASTM D 4375 : 1996 : R2011 Standard Practice for Basic Statistics in Committee D-19 on Water (Withdrawn 2018)
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM D 3856 : 2011 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM D 3648 : 1995 Standard Practices for the Measurement of Radioactivity
ASTM D 5810 : 1996 : R2006 Standard Guide for Spiking into Aqueous Samples
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 3856 : 1995 : R2006 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 2777 : 2008 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM D 2777 : 2006 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3856 : 1995 : R2000 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM D 5810 : 1996 Standard Guide for Spiking into Aqueous Samples
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 2777 : 2008 : EDT 1 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 5810 : 1996 : R2015 Standard Guide for Spiking into Aqueous Samples

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