BS ISO 13547-2:2014
Current
The latest, up-to-date edition.
Copper, lead, zinc and nickel sulfide concentrates. Determination of arsenic Acid digestion and inductively coupled plasma atomic emission spectrometric method
Hardcopy , PDF
English
30-11-2014
Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Sampling and sample preparation
7 Procedure
8 Expression of results
9 Precision
10 Test report
Annex A (normative) - Procedure for the preparation
and determination of the mass of a pre-dried
test portion
Annex B (normative) - Flowsheet of the procedure
for the acceptance of analytical values for
test samples
Defines an acid digestion and inductively coupled plasma atomic emission spectrometric (ICP-AES) method for the determination of the mass fraction of arsenic in copper, lead, zinc, and nickel sulfide concentrates as follows: a) for copper sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05% to 2,0%; b) for lead sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05% to 1,0%; c) for zinc sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05% to 0,6%; and d) for nickel sulfide concentrates, the method is applicable to the determination of mass fraction of arsenic from 0,05% to 1,0%.
| Committee |
W/-
|
| DevelopmentNote |
Supersedes 14/30272868 DC. (11/2014)
|
| DocumentType |
Standard
|
| Pages |
22
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
This International Standard specifies an acid digestion and inductively coupled plasma atomic emission spectrometric (ICP-AES) method for the determination of the mass fraction of arsenic in copper, lead, zinc, and nickel sulfide concentrates as follows: for copper sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05% to 2,0%; for lead sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05% to 1,0%; for zinc sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05% to 0,6%; for nickel sulfide concentrates, the method is applicable to the determination of mass fraction of arsenic from 0,05% to 1,0%.
| Standards | Relationship |
| ISO 13547-2:2014 | Identical |
| ISO 9599:2015 | Copper, lead, zinc and nickel sulfide concentrates — Determination of hygroscopic moisture content of the analysis sample — Gravimetric method |
| ISO 4787:2010 | Laboratory glassware — Volumetric instruments — Methods for testing of capacity and for use |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| ISO 648:2008 | Laboratory glassware — Single-volume pipettes |
| ISO 12743:2006 | Copper, lead, zinc and nickel concentrates — Sampling procedures for determination of metal and moisture content |
| ISO 8466-2:2001 | Water quality — Calibration and evaluation of analytical methods and estimation of performance characteristics — Part 2: Calibration strategy for non-linear second-order calibration functions |
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