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EN 14112:2016

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of oxidation stability (accelerated oxidation test)
Superseded date

07-12-2020

Published date

07-09-2016

European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Sampling
8 Preparation of measurement
9 Measurement
10 Calculation and Evaluation
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Background of the method
Annex B (informative) - Results of an Interlaboratory
        Study
Bibliography

This European Standard specifies a method for the determination of the oxidation stability of fatty acid methyl esters (FAME) at 110 °C, by means of measuring the induction period up to 48 h.NOTE 1EN 15751 [1] describes a similar test method for oxidation stability determination of pure fatty acid methyl esters and of blends of FAME with petroleum-based diesel containing 2 % (V/V) of FAME at minimum.NOTE 2The precision statement of this test method was determined in a Round Robin exercise with induction periods up to 8,5 h, thus covering the limit value in EN 14214. Results from precision studies on EN 15751 indicate that the precision statement is valid for induction periods up to 48 h but not for higher values.NOTE 3Limited studies on EN 15751 with EHN (2-ethyl hexyl nitrate) on FAME blends indicated that the stability is reduced to an extent which is within the reproducibility of the test method. It is likely that the oxidation stability of pure FAMEs is also reduced in the presence of EHN when EN 14112 is used for testing.

Committee
CEN/TC 307
DevelopmentNote
Supersedes PREN 14112. (09/2016)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Superseded
SupersededBy
Supersedes

S.R. CEN/TR 16389:2017 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL AND BLENDS WITH FAME - BACKGROUND TO THE PARAMETERS REQUIRED AND THEIR RESPECTIVE LIMITS AND DETERMINATION
PD CEN/TR 16389:2017 Automotive fuels. Paraffinic diesel fuel and blends with FAME. Background to the parameters required and their respective limits and determination
09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
13/30277078 DC : 0 BS EN 16568 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
BS 2000-574(2014) : 2014 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD
I.S. EN 14213:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
DIN EN 15751 E : 2014 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD
CEN/TR 16366:2012 Liquid petroleum products - Middle distillates and fatty acid methyl ester (FAME) fuels and blends - Round Robin report on applicability of Rapid Small Scale Oxidation Test method
DIN EN 16568 E : 2015 AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
S.R. CWA 16379:2011 FUELS AND BIOFUELS - PURE PLANT OIL FUEL FOR DIESEL ENGINE CONCEPTS - REQUIREMENTS AND TEST METHODS
BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNI EN 15751 : 2014 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD
BS EN 15751:2014 Automotive fuels. Fatty acid methyl ester (FAME) fuel and blends with diesel fuel. Determination of oxidation stability by accelerated oxidation method
DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 15751:2014-06 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD
I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNE-EN 15751:2014 Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation method
BS 2000-620(2014) : 2014 AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
BS EN 16568:2014 Automotive fuels. Blends of Fatty acid methyl ester (FAME) with diesel fuel. Determination of oxidation stability by rapidly accelerated oxidation method at 120 °C
XP M15 032 : 2010 XP AUTOMOTIVE FUELS - FATTY ACID METHYL AND ETHYL ESTERS (FAME AND FAEE) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
DIN EN 16568:2015-03 AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
18/30369065 DC : DRAFT FEB 2018 BS EN 14214 AMD 2 - LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
17/30365049 DC : 0 BS EN 17181 - LUBRICANTS - DETERMINATION OF AEROBIC BIOLOGICAL DEGRADATION OF FULLY FORMULATED LUBRICANTS IN AN AQUEOUS SOLUTION - TEST METHOD BASED ON CO[2]-PRODUCTION
BS EN 14213:2003 Heating fuels. Fatty acid methyl esters (FAME). Requirements and test methods
EN 14213:2003/AC:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
EN 15751:2014 Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation method
EN 16568:2014 Automotive fuels - Blends of Fatty acid methyl ester (FAME) with diesel fuel - Determination of oxidation stability by rapidly accelerated oxidation method at 120 °C
I.S. EN 16568:2014 AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
08/30172824 DC : DRAFT JAN 2008 BS EN 15751 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD
PD CEN/TR 16366:2012 Liquid petroleum products. Middle distillates and fatty acid methyl ester (FAME) fuels and blends. Round Robin report on applicability of Rapid Small Scale Oxidation Test method
12/30268200 DC : 0 BS EN 15751 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD
S.R. CEN/TR 16366:2012 LIQUID PETROLEUM PRODUCTS - MIDDLE DISTILLATES AND FATTY ACID METHYL ESTER (FAME) FUELS AND BLENDS - ROUND ROBIN REPORT ON APPLICABILITY OF RAPID SMALL SCALE OXIDATION TEST METHOD
BS 2000-574(2009) : 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD
UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
ASTM D 7467 : 2017-03 SPECIFICATION FOR DIESEL FUEL OIL, BIODIESEL BLEND (B6 TO B20)
I.S. EN 15751:2014 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD
DIN EN 14213 E : 2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14213:2003-11 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
CEN/TR 16389:2017 Automotive fuels - Paraffinic diesel fuel and blends with FAME - Background to the parameters required and their respective limits and determination

ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 6886:2016 Animal and vegetable fats and oils Determination of oxidative stability (accelerated oxidation test)
EN ISO 6886:2016 ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF OXIDATIVE STABILITY (ACCELERATED OXIDATION TEST) (ISO 6886:2016)
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN 15751:2014 Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation method
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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