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EN 14582:2016

Current
Current

The latest, up-to-date edition.

Characterization of waste - Halogen and sulfur content - Oxygen combustion in closed systems and determination methods
Published date

03-08-2016

European Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Hazards
7 Reagents and control mixtures
8 Sample conservation and pretreatment of test portion
9 Equipment
10 Procedure
11 Recommended methods of determination
12 Control measurements
13 Evaluation
14 Test report
Annex A (informative) - Performance characteristics
Annex B (informative) - Oxygen flask combustion by
        Schoeniger
Annex C (informative) - Recovery yields obtained for
        control mixtures with different absorption
        solutions and analytical techniques
Annex D (informative) - Examples of possible control
        substances
Annex E (informative) - Additional results of
        inter-laboratory tests
Annex F (informative) - Summary of general
        requirements and recommendations
Annex G (informative) - Additional validation data
Bibliography

This standard specifies a combustion method for the determination of halogen and sulfur contents in materials by combustion in a closed system containing oxygen (calorimetric bomb), and the subsequent analysis of the combustion product using different analytical techniques.This method is applicable to solid, pasty and liquid samples containing more than 0,025 g/kg of halogen and/or 0,025 g/kg of sulfur content. The limit of detection depends on the element, the matrix and the determination technique used.Insoluble halides and sulphate present in the sample or produced during the combustion step are not completely determined by these methods.

Committee
CEN/TC 444
DevelopmentNote
Supersedes PREN 14582. (08/2016)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

Standards Relationship
NBN EN 14582 : 2007 Identical
SS-EN 14582:2016 Identical
UNE-EN 14582:2016 Identical
DIN EN 14582 E : 2016 Identical
NS EN 14582 : 2007 Identical
NF EN 14582 : 2016 Identical
BS EN 14582:2007 Identical
NEN EN 14582 : 2016 Identical
PN EN 14582 : 2017 Identical
I.S. EN 14582:2016 Identical
DIN EN 14582:2015-04 (Draft) Identical
SN EN 14582:2016 Identical
UNI EN 14582 : 2007 Identical
UNI EN 14582:2016 Identical
DIN EN 14582:2016-12 Identical
BS EN 14582:2016 Identical

PD CEN/TR 16376:2012 Characterization of waste. Overall guidance document for characterization of waste from the extractive industries
PD CLC/TS 50625-3-1:2015 Collection, logistics & treatment requirements for WEEE Specification for de-pollution. General
IEC PAS 63015:2016 Definition of "Low-Halogen" for electronic products
CEN/TR 16376:2012 Characterization of waste - Overall guidance document for characterization of waste from the extractive industries
EN 15875:2011/AC:2012 CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
IPC J STD 004 RUSSIAN : B REQUIREMENTS FOR SOLDERING FLUXES
IPC J STD 004 CHINESE : B REQUIREMENTS FOR SOLDERING FLUXES
10/30229134 DC : 0 BS EN 62321-3-2 ED 1 - DETERMINATION OF CERTAIN SUBSTANCES IN ELECTROTECHNICAL PRODUCTS - PART 3-2: SCREENING OF TOTAL BROMINE IN ELECTRIC AND ELECTRONIC PRODUCTS BY COMBUSTION - ION CHROMATOGRAPHY (C-IC)
UNI EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
I.S. EN 50642:2018 CABLE MANAGEMENT SYSTEMS - TEST METHOD FOR CONTENT OF HALOGENS
I.S. EN 16457:2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
EN 50642:2018 Cable management systems - Test method for content of halogens
S.R. CEN/TR 16376:2012 CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
UNE-EN 15289:2011 Solid biofuels - Determination of total content of sulfur and chlorine
17/30348303 DC : 0 BS EN 17087 - CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE FOR TESTING OF RELEASE AND ANALYSIS OF CONTENT
UNE-EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
I.S. EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
BS EN 15289:2011 Solid biofuels. Determination of total content of sulfur and chlorine
BS EN 62321-3-2:2014 Determination of certain substances in electrotechnical products Screening. Total bromine in polymers and electronics by Combustion. Ion Chromatography
BS EN 15875:2011 Characterisation of waste. Static test for determination of acid potential and neutralisation potential of sulfidic waste
PREN 50642 : DRAFT 2016 CABLE MANAGEMENT SYSTEMS - TEST METHOD FOR CONTENT OF HALOGENS
I.S. EN ISO 16994:2016 SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE (ISO 16994:2016)
UNE-EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
UNI EN 15289 : 2011 SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE
DIN EN 15875 E : 2012 CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
I.S. EN 15875:2011 CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
DIN EN 15875:2012-11 Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste (includes Corrigendum :2012)
13/30277477 DC : 0 BS EN ISO 16994 - SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULPHUR AND CHLORINE
S.R. CLC/TS 50625-3-1:2015 COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-1: SPECIFICATION FOR DE-POLLUTION - GENERAL
DIN EN 15289:2011-04 SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE
12/30263896 DC : 0 BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
UNI EN 15875 : 2011 CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
DIN EN 16457:2014-07 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
I.S. EN 62321-3-2:2014 DETERMINATION OF CERTAIN SUBSTANCES IN ELECTROTECHNICAL PRODUCTS - PART 3-2: SCREENING - TOTAL BROMINE IN POLYMERS AND ELECTRONICS BY COMBUSTION - ION CHROMATOGRAPHY
13/30291099 DC : 0 BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
17/30350920 DC : 0 BS EN 63031 - DEFINITION OF LOW HALOGEN MATERIALS USED IN ELECTRONIC AND ELECTRICAL PRODUCTS
ISO 16994:2016 Solid biofuels — Determination of total content of sulfur and chlorine
PD IEC/PAS 63015:2016 Definition of “Low-Halogen?? for electronic products
DIN EN 15002:2015-07 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
IPC J STD 004 : B REQUIREMENTS FOR SOLDERING FLUXES
EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
EN ISO 16994:2016 Solid biofuels - Determination of total content of sulfur and chlorine (ISO 16994:2016)
CLC/TS 50625-3-1:2015 Collection, logistics & treatment requirements for WEEE - Part 3-1: Specification for de-pollution - General
BS EN ISO 16994:2015 Solid biofuels. Determination of total content of sulfur and chlorine
DIN EN 16457 E : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
10/30219387 DC : 0 BS EN 15289 - SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULPHUR AND CHLORINE
NF EN 15875 : 2011 CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE
BS EN 16457:2014 Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report
UNE-EN 15875:2012 Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste
08/30189276 DC : 0 BS EN 15875 - CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL OF SULFIDIC WASTE
16/30331003 DC : 0 BS EN 50642 - CABLE MANAGEMENT SYSTEMS - TEST METHOD FOR CONTENT OF HALOGENS
I.S. EN 15289:2011 SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE
CSA ISO 16994 : 2015 SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE
DIN EN 15002 E : 2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
BS EN 15002:2015 Characterization of waste. Preparation of test portions from the laboratory sample
EN 62321-3-2:2014 Determination of certain substances in electrotechnical products - Part 3-2: Screening - Total bromine in polymers and electronics by Combustion - Ion Chromatography
EN 15289:2011 Solid biofuels - Determination of total content of sulfur and chlorine

EN ISO 11885:2009 Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (ISO 11885:2007)
EN ISO 10304-3 : 1997 Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 3: Determination of chromate, iodide, sulfite, thiocyanate and thiosulfate (ISO 10304-3:1997)
ASTM D 808 : 2016 : REDLINE Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method)
ISO 10304-3:1997 Water quality — Determination of dissolved anions by liquid chromatography of ions — Part 3: Determination of chromate, iodide, sulfite, thiocyanate and thiosulfate
EN 14346:2006 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
ISO 9297:1989 Water quality Determination of chloride Silver nitrate titration with chromate indicator (Mohr's method)
ISO 11885:2007 Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)
ISO 10304-1:2007 Water quality Determination of dissolved anions by liquid chromatography of ions Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate
ISO 10304-2:1995 Water quality Determination of dissolved anions by liquid chromatography of ions Part 2: Determination of bromide, chloride, nitrate, nitrite, orthophosphate and sulfate in waste water
ISO 10359-1:1992 Water quality — Determination of fluoride — Part 1: Electrochemical probe method for potable and lightly polluted water
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
ASTM E 442 : 1991 Test Method for Chlorine, Bromine, or Iodine in Organic Compounds by Oxygen Flask Combustion (Withdrawn 1997)
EN ISO 10304-1:2009 Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate (ISO 10304-1:2007)

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