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PREN 16167 : DRAFT 2017

Current
Current

The latest, up-to-date edition.

SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
Published date

12-01-2013

European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Safety remarks
7 Reagents
8 Apparatus
9 Sample storage and preservation
10 Procedure
11 Performance characteristics
12 Precision
13 Test report
Annex A (informative) - Repeatability and
        reproducibility data
Annex B (informative) - Examples for
        retention times of PCBs
Annex C (informative) - Calculation method for
        the estimation of total PCB content
Bibliography

Defines the method for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180) in sludge, treated biowaste and soil using GC-MS and GC-ECD.

Committee
TC 444
DocumentType
Draft
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
NEN EN 16167 : 2018 Identical
17/30364002 DC : DRAFT OCT 2017 Identical
DIN EN 16167:2012-11 Identical
NEN EN 16167 : 2012 Identical
17/30364002 DC : 0 Identical
10/30147454 DC : 0 Identical

EN ISO 6468 : 1996 WATER QUALITY - DETERMINATION OF CERTAIN ORGANOCHLORINE INSECTICIDES, POLYCHLORINATED BIPHENYLS AND CHLOROBENZENES - GAS CHROMATOGRAPHIC METHOD AFTER LIQUID-LIQUID EXTRACTION
EN 12766-1:2000 Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)
ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
EN 61619:1997 Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography
EN 15308:2016 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
ISO 5667-15:2009 Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples
EN ISO 16720:2007 Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005)
EN 12766-2:2001 Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
EN ISO 5667-15:2009 Water quality - Sampling - Part 15: Guidance on the preservation and handling of sludge and sediment samples (ISO 5667-15:2009)
EN 15934:2012 Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content
EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment
CEN/TS 16181:2013 Sludge, treated biowaste and soil - Determination of polycyclic aromatic hydrocarbons (PAH) by gas chromatography (GC) and high performance liquid chromatography (HPLC)
ISO 18512:2007 Soil quality Guidance on long and short term storage of soil samples

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