PREN 16190 : DRAFT 2017
Current
The latest, up-to-date edition.
SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
28-11-2017
European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Abbreviations
5 Principle
6 Reagents
7 Apparatus and materials
8 Sample storage and sample pretreatment
9 Extraction and clean-up
10 HRGC/HRMS analysis
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Toxic equivalency
factor (TEF)
Annex B (informative) - Examples of extraction
and clean-up methods
Annex C (informative) - Examples of operation of
GC/HRMS determination - Example
Annex D (informative) - Repeatability and reproducibility
data
Bibliography
Describes the method for quantitative determination of 17 2,3,7,8-chlorine substituted dibenzo-p-dioxins and dibenzofurans and dioxin-like polychlorinated biphenyls in sludge, treated biowaste and soil using liquid column chromatographic clean-up methods and GC/HRMS.
| Committee |
TC 444
|
| DocumentType |
Draft
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Standards | Relationship |
| 17/30363999 DC : DRAFT OCT 2017 | Identical |
| NEN EN 16190 : DRAFT 2017 | Identical |
| DIN EN 16190:2017-11 (Draft) | Identical |
| NF EN 16190 : 2017 PR | Identical |
| 17/30363999 DC : 0 | Identical |
| EN 1948-2:2006 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs |
| EN 1948-1:2006 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs |
| EN 1948-3:2006 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs |
| ISO 18073:2004 | Water quality — Determination of tetra- to octa-chlorinated dioxins and furans — Method using isotope dilution HRGC/HRMS |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| EN 15934:2012 | Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content |
| EN 16179:2012 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |