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ASTM D 6234 : 2013

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Shake Extraction of Mining Waste by the Synthetic Precipitation Leaching Procedure

Available format(s)

Hardcopy , PDF

Superseded date

12-09-2020

Language(s)

English

Published date

01-09-2013

This test method covers a procedure for the shake leaching of mining waste containing at least 80 % dry solids (≤20 % moisture) in order to generate a solution to be used to determine the inorganic constituents leached under the specified testing conditions that conform to the synthetic precipitation leaching procedure (SPLP).

1.1This test method covers a procedure for the shake leaching of mining waste containing at least 80 % dry solids (20 % moisture) in order to generate a solution to be used to determine the inorganic constituents leached under the specified testing conditions that conform to the synthetic precipitation leaching procedure (SPLP).

1.2This test method calls for the shaking of a known weight of mining waste with acidic extraction fluid of a specified composition as well as the separation of the liquid phase for analysis. The pH of the extraction fluid is to reflect the pH of acidic precipitation in the geographic region in which the waste being tested is to be disposed.

Note 1Possible sources of information concerning the pH of the precipitation in the geographic region of interest include state and federal environmental agencies, state universities, libraries, etc. pH values given in USEPA Method 1312, that are 4.2 east of the Mississippi River and 5.0 west of the Mississippi River and are based on acid precipitation maps, are examples of values that can be used. If the pH of the laboratory water is less than the desired pH for the site, do not use this test method; use Test Method D3987 or Test Method E2242.
Note 2The method may also be suitable for use in testing of mineral processing waste from meal mining process operations for jurisdictions that do not require the use of Test Method E2242.

1.3This test method is intended to describe the procedure for performing single batch extractions only. It does not describe all types of sampling, sample preservation, and analytical requirements that may be associated with its application.

1.4The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
D 34
DocumentType
Test Method
Pages
7
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 8155 : 2017 Standard Practice for Shake Extraction of Solid Mining and Metallurgical Processing Waste with Water
ASTM E 2242 : 2013 Standard Test Method for Column Percolation Extraction of Mine Rock by the Meteoric Water Mobility Procedure
ASTM E 1915 : 2013 Standard Test Methods for Analysis of Metal Bearing Ores and Related Materials for Carbon, Sulfur, and Acid-Base Characteristics
ASTM D 8187 : 2018 Standard Guide for Interpretation of Standard Humidity Cell Test Results

ASTM E 2242 : 2002 Standard Test Method for Column Percolation Extraction of Mine Rock by the Meteoric Water Mobility Procedure
ASTM E 1915 : 2007 : REV A Standard Test Methods for Analysis of Metal Bearing Ores and Related Materials by Combustion Infrared-Absorption Spectrometry
ASTM D 5744 : 2007 : EDT 1 Standard Test Method for Laboratory Weathering of Solid Materials Using a Humidity Cell
ASTM D 3370 : 1995 : REV A : R2003 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM D 5744 : 2013 Standard Test Method for Laboratory Weathering of Solid Materials Using a Humidity Cell
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM E 1915 : 1999 Standard Test Method for Analysis of Metal Bearing Ores and Related Materials by Combustion Infrared Absorption Spectrometry
ASTM D 2777 : 2012 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM D 5744 : 1996 Standard Test Method for Accelerated Weathering of Solid Materials Using a Modified Humidity Cell
ASTM D 2777 : 2003 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
ASTM D 3370 : 2010 Standard Practices for Sampling Water from Closed Conduits
ASTM D 2777 : 2013 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 5744 : 2012 Standard Test Method for Laboratory Weathering of Solid Materials Using a Humidity Cell
ASTM E 1915 : 2005 Standard Test Methods for Analysis of Metal Bearing Ores and Related Materials by Combustion Infrared Absorption Spectrometry
ASTM D 2777 : 1998 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
ASTM D 3370 : 2008 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM E 1915 : 2009 Standard Test Methods for Analysis of Metal Bearing Ores and Related Materials for Carbon, Sulfur, and Acid-Base Characteristics
ASTM E 1915 : 2001 Standard Test Methods for Analysis of Metal Bearing Ores and Related Materials by Combustion Infrared Absorption Spectrometry
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 3987 : 1985 : R1999 Standard Test Method for Shake Extraction of Solid Waste with Water
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM E 2242 : 2007 Standard Test Method for Column Percolation Extraction of Mine Rock by the Meteoric Water Mobility Procedure
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 5744 : 2013 : EDT 1 Standard Test Method for Laboratory Weathering of Solid Materials Using a Humidity Cell
ASTM D 3987 : 2012 Standard Practice for Shake Extraction of Solid Waste with Water
ASTM E 1915 : 2011 Standard Test Methods for Analysis of Metal Bearing Ores and Related Materials for Carbon, Sulfur, and Acid-Base Characteristics
ASTM E 1915 : 2013 Standard Test Methods for Analysis of Metal Bearing Ores and Related Materials for Carbon, Sulfur, and Acid-Base Characteristics
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 2777 : 2008 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 2777 : 2006 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM E 2242 : 2013 Standard Test Method for Column Percolation Extraction of Mine Rock by the Meteoric Water Mobility Procedure
ASTM D 3370 : 2018 Standard Practices for Sampling Water from Flowing Process Streams
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 3370 : 1976 Standard Practices for Sampling Water
ASTM E 2242 : 2012 : REV A Standard Test Method for Column Percolation Extraction of Mine Rock by the Meteoric Water Mobility Procedure
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 5744 : 2007 Standard Test Method for Laboratory Weathering of Solid Materials Using a Humidity Cell
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 3370 : 1995 : REV A : R1999 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
ASTM E 2242 : 2012 : EDT 1 Standard Test Method for Column Percolation Extraction of Mine Rock by the Meteoric Water Mobility Procedure
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM D 3370 : 2007 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 3987 : 1985 : R2004 Standard Test Method for Shake Extraction of Solid Waste with Water
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
ASTM D 3987 : 2006 Standard Test Method for Shake Extraction of Solid Waste with Water
ASTM D 5744 : 2018 Standard Test Method for Laboratory Weathering of Solid Materials Using a Humidity Cell
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 2777 : 2008 : EDT 1 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3987 : 2012 : R2020 Standard Practice for Shake Extraction of Solid Waste with Water

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