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EN 15890:2010

Current

Current

The latest, up-to-date edition.

Foodstuffs - Determination of patulin in fruit juice and fruit based purée for infants and young children - HPLC method with liquid/liquid partition cleanup and solid phase extraction and UV detection

Published date

29-09-2010

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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Procedure
7 HPLC analysis
8 Calculation
9 Precision
10 Test report
Annex A (informative) - Typical chromatograms
Annex B (informative) - Precision data
Bibliography

This European Standard specifies a method for the determination of patulin in fruit juices and fruit-based purée, such as baby food purée, using high performance liquid chromatography with ultra-violet detection (HPLC-UV). Using naturally contaminated and spiked samples this method has been validated for the determination of patulin in apple juice, at levels ranging from 3,0 μg/kg to 15,5 μg/kg, and in fruit-based baby food purée, at levels ranging from 3,4 μg/kg to 17,9 μg/kg. Baby food fruit purée (commercially available on the European market) used in this study contained the following ingredients: blueberry; apple; banana; lemon; wheat biscuits; wheat syrup; whole milk; and vegetable oil. A detailed listing, including the fractions, of each product used in this study is given in [1].Further information on validation, see Clause 9 and Annex B.

Committee
CEN/TC 275
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
DIN EN 15890:2010-12 Identical
NBN EN 15890 : 2010 Identical
NF EN 15890 : 2010 Identical
NEN EN 15890 : 2010 Identical
PN EN 15890 : 2012 Identical
I.S. EN 15890:2010 Identical
NS EN 15890 : 1ED 2010 Identical
BS EN 15890:2010 Equivalent
UNE-EN 15890:2011 Identical

ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)

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