EN ISO 22032:2009
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Water quality - Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge - Method using extraction and gas chromatography/mass spectrometry (ISO 22032:2006)
25-02-2009
31-08-2009
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents and standards
6 Apparatus
7 Sampling and sample pre-treatment
8 Procedure
9 Calibration
10 Test report
Annex A (informative) - Clean-up procedures
Annex B (informative) - Examples for separation conditions
in gas chromatography and mass spectrometry
Annex C (informative) - Typical ions and time windows for
electron impact ionization detection
Annex D (informative) - Examples of chromatograms and spectra
Annex E (informative) - Precision data
Bibliography
ISO 22032:2006 specifies a method for the determination of selected polybrominated diphenyl ethers (PBDE) in sediment and sludge using gas chromatography/mass spectrometry (GC-MS) in the electron impact (EI) or negative ion chemical ionization (NCI) mode. When using GC-EI-MS, the method is applicable to samples containing 0,05 to 25 micrograms per kilogram of tetra- to octabromo congeners and 0,3 to 100 micrograms per kilogram of decabromo diphenyl ether (BDE-209), respectively.
| Committee |
CEN/TC 230
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Withdrawn
|
| Standards | Relationship |
| NEN EN ISO 22032 : 2009 | Identical |
| I.S. EN ISO 22032:2009 | Identical |
| SS-EN ISO 22032:2009 | Identical |
| BS EN ISO 22032:2009 | Identical |
| PN EN ISO 22032 : 2009 | Identical |
| NBN EN ISO 22032 : 2009 | Identical |
| DIN EN ISO 22032:2009-07 | Identical |
| NS EN ISO 22032 : 2009 | Identical |
| ISO 22032:2006 | Identical |
| BS 6068-2.99(2006) : 2006 | Identical |
| UNE-EN ISO 22032:2009 | Identical |
| DIN EN 16694:2015-12 | WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) |
| CEN/TR 16417:2016 | Footwear - Footwear industry guideline for substances of very high concern (Annex XIV of REACH) |
| 13/30291096 DC : 0 | BS EN 16694 - WATER QUALITY - DETERMINATION OF PENTABROMODIPHENYL ETHER (PBDE) IN WHOLE WATER SAMPLES USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS) |
| S.R. CEN/TR 16417:2016 | FOOTWEAR - FOOTWEAR INDUSTRY GUIDELINE FOR SUBSTANCES OF VERY HIGH CONCERN (ANNEX 14 OF REACH) |
| BS EN 16377:2013 | Characterization of waste. Determination of brominated flame retardants (BFR) in solid waste |
| DIN EN 16377:2013-12 | Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste |
| PD CEN/TR 16417:2016 | Footwear. Footwear industry guideline for substances of very high concern (Annex XIV of REACH) |
| EN 16694:2015 | Water quality - Determination of selected polybrominated diphenly ether (PBDE) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography - mass spectrometry (GC-MS) |
| EN 16377:2013 | Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste |
| BS EN 16694:2015 | Water quality. Determination of selected polybrominated diphenly ether (PBDE) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography-mass spectrometry (GC-MS) |
| I.S. EN 16694:2015 | WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENYL ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS) |
| 12/30255723 DC : 0 | BS EN 16377 - CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE |
| I.S. EN 16377:2013 | CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE |
| UNE-EN 16377:2014 | Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste |
| UNE-EN 16694:2016 | Water quality - Determination of selected polybrominated diphenly ether (PBDE) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography - mass spectrometry (GC-MS) |
| ISO 5667-13:2011 | Water quality — Sampling — Part 13: Guidance on sampling of sludges |
| ISO/TR 13530:1997 | Water quality — Guide to analytical quality control for water analysis |
| EN 12880:2000 | Characterization of sludges - Determination of dry residue and water content |
| DIN 32645:2008-11 | CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ISO 8466-1:1990 | Water quality — Calibration and evaluation of analytical methods and estimation of performance characteristics — Part 1: Statistical evaluation of the linear calibration function |