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EN 15779:2009+A1:2013

Current
Current

The latest, up-to-date edition.

Petroleum products and fat and oil derivates - Fatty acid methyl esters (FAME) for diesel engines - Determination of polyunsaturated (≥4 double bonds) fatty acid methyl esters (PUFA) by gas chromatography
Published date

25-09-2013

Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Apparatus
5 Reagents and materials
6 Sampling
7 Procedure
8 Calculation
9 Expression of results
10 Precision
11 Test report
Bibliography

This European Standard specifies a method for the determination of the polyunsaturated (≥ 4 double bonds) fatty acid (PUFA) methyl esters content of fatty acid methyl ester (FAME) as a whole between 0,6 % (m/m) and 1,5 % (m/m).The method covers the predominant four polyunsaturated fatty acid methyl esters of eicosatetraenoic acid (C 20:4 (n-6)), eicosapentaenoic acid (C 20:5 (n-3)), docosapentaenoic acid (C 22:5 (n 3), and docosahexaenoic acid (C 22:6 (n 3)). Studies have indicated that based on the linearity of results from this European Standard, PUFA methyl esters can be determined in FAME in the range between 0,3 % (m/m) to 3,0 % (m/m). However, the precision was not established in that range, as no samples within the upper ranges where included in the final interlaboratory test (see 10.1).Although the method is applicable to all uses, it is predominantly for FAME for use in diesel engines.NOTE 1For the purposes of this document, the term “% (m/m)” is used to represent the mass fraction of a material.NOTE 2This European Standard is based on A.O.C.S Official Method Ce 1b-89 [1].

Committee
CEN/TC 19
DevelopmentNote
2009 Edition Re-Issued in September 2013 & incorporates AMD 1 2013. (10/2013)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
PD ISO/TS 17307:2016 Petroleum products. Biodiesel. Determination of total esters content by gas chromatography
I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
ISO/TS 17307:2016 Petroleum products — Biodiesel — Determination of total esters content by gas chromatography
UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
18/30369065 DC : DRAFT FEB 2018 BS EN 14214 AMD 2 - LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS

ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN ISO 5509 : 2000 ANIMAL AND VEGETABLE FATS AND OILS - PREPARATION OF METHYL ESTER OF FATTY ACIDS
ISO 5509:2000 Animal and vegetable fats and oils Preparation of methyl esters of fatty acids
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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