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ASTM D 1266 : 2018

Current

Current

The latest, up-to-date edition.

Standard Test Method for Sulfur in Petroleum Products (Lamp Method)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-04-2018

This test method covers the determination of total sulfur in liquid petroleum products in concentrations from 0.01 % to 0.4 % by mass (Note 1).

Committee
D 02
DocumentType
Test Method
Pages
12
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This test method covers the determination of total sulfur in liquid petroleum products in concentrations from 0.01 % to 0.4 % by mass (Note 1). A special sulfate analysis procedure is described in Annex A1 that permits the determination of sulfur in concentrations as low as 5 mg/kg.

Note 1:The comparable lamp method for the determination of sulfur in liquefied petroleum gas is described in Test Method D2784. For the determination of sulfur in heavier petroleum products that cannot be burned in a lamp, see the high pressure decomposition device method (Test Method D129) the quartz tube method (IP 63), or the high-temperature method (Test Method D1552).

1.2The direct burning procedure (Section 9) is applicable to the analysis of such materials as gasoline, kerosine, naphtha, and other liquids that can be burned completely in a wick lamp. The blending procedure (Section 10) is applicable to the analysis of gas oils and distillate fuel oils, naphthenic acids, alkyl phenols, high sulfur content petroleum products, and many other materials that cannot be burned satisfactorily by the direct burning procedure.

1.3Phosphorus compounds normally present in commercial gasoline do not interfere. A correction is given for the small amount of acid resulting from the combustion of the lead anti-knock fluids in gasolines. Appreciable concentrations of acid-forming or base-forming elements from other sources interfere when the titration procedure is employed since no correction is provided in these cases.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 2784 : 1989 Standard Test Method for Sulfur in Liquefied Petroleum Gases (Oxy-Hydrogen Burner or Lamp)
ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2017 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6299 : 2009 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1552 : 2008 : R2014 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6300 : 2017 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 6299 : 2013 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6792 : 2006 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1552 : 1990 : EDT 1 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM E 11 : 2024 Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves
ASTM D 6792 : 2004 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
ASTM D 1552 : 2016 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conducitivity Detection (TCD)
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 6299 : 2010 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2022 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2016 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 6300 : 2004 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 1552 : 2000 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D 6792 : 2021 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2023 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6300 : 2019 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6299 : 2023 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6792 : 2004 : REV A Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
ASTM D 6300 : 2021 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2019 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6792 : 2005 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
ASTM D 6300 : 2023 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2020 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2010 : EDT 2 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2016 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM E 11 : 2022 Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves
ASTM D 6792 : 2023 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 1552 : 2023 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 6300 : 2023 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6792 : 2020 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2019 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6792 : 2021 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6300 : 2020 : REV B Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 6299 : 2023 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2000 : REV A Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2006 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6792 : 2013 Standard Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories
ASTM D 2784 : 2006 Standard Test Method for Sulfur in Liquefied Petroleum Gases (Oxy-Hydrogen Burner or Lamp)
ASTM D 6792 : 2017 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6300 : 2014 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6300 : 2015 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 1552 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 1552 : 2007 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D 6300 : 1999 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6792 : 2007 Standard Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories
ASTM D 4177 : 2022 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 1552 : 1995 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D 6792 : 2021 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2023 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2020 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 1552 : 2015 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and IR Detection
ASTM D 1552 : 2001 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D 6299 : 2008 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6792 : 2023 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
ASTM D 1552 : 2008 : R2014 : EDT 1 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D 2784 : 2011 Standard Test Method for Sulfur in Liquefied Petroleum Gases (Oxy-Hydrogen Burner or Lamp) (Withdrawn 2016)
ASTM D 6300 : 2013 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6299 : 2002 : EDT 1 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2008 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6300 : 2003 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6300 : 2007 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 6299 : 2022 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6792 : 2022 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6300 : 2002 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 1552 : 2008 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 6792 : 2003 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
ASTM D 4177 : 2020 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 6300 : 2016 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 6792 : 2002 Standard Guide for A Quality System in Petroleum Products and Lubricants Testing Laboratories
ASTM D 6299 : 2007 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6792 : 2023 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6299 : 2007 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4177 : 2022 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 1552 : 2016 : R2021 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 6299 : 2017 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6792 : 2022 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6300 : 2014 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 1552 : 1983 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D 2784 : 1998 Standard Test Method for Sulfur in Liquefied Petroleum Gases (Oxy-Hydrogen Burner or Lamp)
ASTM D 6299 : 2002 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6300 : 2024 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants

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